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The system was set to a flow rate of 0.060 mL/min and composed of 5 mM ammonium formate in a gradient of water/acetonitrile concentrations (all mobile phase solvents were Optima LC/MS Grade, and purchased from Fisher Scientific, Fair Lawn, NJ)
Eur J Obstet Gynecol Reprod Biol 2005;119:606
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