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Research on Flammulina velutipes fruiting bodies examined the impact of refrigeration on nutritional content and active ingredients, revealing a significant decline in the natural antioxidant L-ergothioneine concentration after 8 days at 5C in both bright and dark conditions, while total phenolic content increased notably over 10 days of refrigeration under fluorescent lighting

Bousfiha A, Jeddane L, Picard C, Al-Herz W, Ailal F, Chatila T, et al

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If you still see undissolved powder, gently swirl again

The problem is extended room-temperature storage, repeated warming, leaving the vial on a bench, or shipping and storing reconstituted solution outside a controlled cold chain

There are also multiple detoxification pathways for many of the toxins that glutathione helps remove