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The supernatants were collected and put on ice until measurement

Yes, and it is increasingly common

The Three Failure Modes of Compounded Reconstitution After reviewing reconstitution issues reported to FormBlends clinical support over 18 months, three failure patterns account for 94% of unusable vials: Failure Mode 1: Mechanical denaturation (foam and aggregates)

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However, limited affordability and healthcare infrastructure challenges slow uptake in lower-income areas