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The salt according to claim 1 or 2 wherein Xaa is Ala, bAla, Leu, Ile, Gly, Val, Nle or Nva, Yaa is Lys, Arg, Orn or His and Zaa is Glu, Asp, Aad or Apm

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Briefly, metabolites in plasma (100 L) were extracted with 90% methanol (900 L), and proteins were precipitated at -20 C for 2 h, followed by centrifugation for 10 min at 4000 rpm at 4 C